Research article - Peer-reviewed, 2022
Complete H-1 and C-13 NMR spectral assignment of D-glucofuranose
Alexandersson, Elin; Nestor, Gustav;Abstract
Although D-glucose is the most common sugar in nature, only a few NMR studies have focused on its minor furanose forms, and they have been limited to the anomeric position. Here, complete H-1 and C-13 NMR spectral analysis of alpha- and beta-D-glucofuranose was performed, including signal assignment, chemical shifts, and coupling constants. Selective and non-selective 1D and 2D NMR experiments were used for the analysis, complemented by spin simulations and iterative spectral analysis.
Keywords
Glucose; Furanose; Glucofuranose; NMR spectroscopy; Selective NMR experiment; Coupling constants
Published in
Carbohydrate Research 2022, volume: 511, article number: 108477Publisher: ELSEVIER SCI LTD
Authors' information
Swedish University of Agricultural Sciences, Department of Molecular Sciences
Swedish University of Agricultural Sciences, Department of Molecular Sciences
UKÄ Subject classification
Biochemistry and Molecular Biology
Publication Identifiers
DOI: https://doi.org/10.1016/j.carres.2021.108477
URI (permanent link to this page)
https://res.slu.se/id/publ/114515